Extraction and Characterization of Cola Millenii K. Schum (Monkey Cola) Seed Oil: Optimization Using Full Factorial Design of Experiment

Contenu principal de l'article

Elizabeth Ogbeh
Emmanuel Gimba Casmir
Abdulkadir Nuhu Abdulmumin
Eyije Abechi Stephen
Risikat Agbeke Iyun Ogunkemi

Résumé

Plant seed oils are vital sources of oil of nutritional, pharmaceutical and industrial importance. Presently the quest for plant seed oils has increased greatly due to the diverse application of these oils. Hence the need for low-cost oil seed crop to produce inexpensive oils to meet these needs. This work focuses on the solvent extraction of oil from Cola millenii seeds. The extraction process was optimized using a 2-level full factorial design of experiment in terms of oil yield to determine the optimum extraction conditions. Based on the design, 8 experiments were carried out with three varying parameters: solvent volume, extraction time and sample weight. A first order regression equation best fits the experimental data. The predicted values calculated by the regression model were in good agreement with the experimental values. From our results, the condition for obtaining the optimum yield (2.71%) of the seed oil was attained when 50.00 g of the pulverized seed sample was extracted with 200.00 cm3 n-hexane for 60 minutes. The oil has peroxide value 35.00meqKOH/g, acid value 32.00mgKOH/g, iodine value 96.57gI2/100g and FFA 16.09%. These values obtained were in agreement with the values reported for oils which find use in the cosmetics and paint industries.

Téléchargements

Les données relatives au téléchargement ne sont pas encore disponibles.

Renseignements sur l'article

Comment citer
Ogbeh, E., Casmir, E. G., Abdulmumin, A. N., Stephen, E. A., & Ogunkemi, R. A. I. (2018). Extraction and Characterization of Cola Millenii K. Schum (Monkey Cola) Seed Oil: Optimization Using Full Factorial Design of Experiment. Nigerian Journal of Pharmaceutical and Applied Science Research, 7(2), 1–6. Consulté à l’adresse https://nijophasr.net/index.php/nijophasr/article/view/209
Rubrique
Articles
Bibliographies de l'auteur-e

Elizabeth Ogbeh

Department Of Chemistry, Ahmadu Bello University, Zaria, Nigeria

Emmanuel Gimba Casmir

Department Of Chemistry, Ahmadu Bello University, Zaria, Nigeria

Abdulkadir Nuhu Abdulmumin

Department Of Chemistry, Ahmadu Bello University, Zaria, Nigeria

Eyije Abechi Stephen

Department Of Chemistry, Ahmadu Bello University, Zaria, Nigeria

Risikat Agbeke Iyun Ogunkemi

Department Of Chemistry, Ahmadu Bello University, Zaria, Nigeria

Références

A.O.A.C. (1990).Official methods of analysis of the association of official analytical chemists. 15th Ed., Washington DC, USA: Association of Official Chemists.

Adegoke E, Akinsanya A, Nagu A, (1968). Studies of Nigerian medicinal plants.A preliminary surve of plant alkaloids. Journal of the West African Science Association.13: 13-39.

Adenyi BA, Groove MJ, Gangaharan PRT, (2004). In vitro antimyco bacteria activities of three species of cola plant extracts (sterculiacea). Phytotherapy Research. 18(5): 414-418.

Adepoju TF, Olawale O, Abiodun AO, (2013). Optimization, kinetic degradation and quality characterization of oil extracted from Nigeria Hibiscus sabdariffa oil seeds. International Journal of Engineering Research and Technology. 2(11): 3856-3875.

Akanni MS, Adekunle AS, Oluyemi EA, (2001). Physicochemical properties of some non-conventional oil seeds. Journal of food technology. 3(2): 177-181.

Alkantara A, Amores J, Canoira L, Fidalgo E, Franco MJ, Navarro A, (2000).Catalytic production of biodiesel from soyabean oil used as frying oil and tallow. Biomass & Bioenergy.18: 515-527.

Aremu M O, Ibrahim H, and Bamidele T O, (2015). Physicochemical Characteristics of the Oils Extracted from Some Nigerian Plant Foods – A Review, Chemical and Process Engineering Research. 32, 36-52.

Dorado MP, Ballesteros E, Lopez FJ, Mittelbach M, (2004). Optimization of alkali catalyzed transesterification of Bassica carinata oil for biodiesel production. Energy and Fuels.18: 77-83.

Eromosele CC, Eromosele CO, Akintoye AO, Komolafe TO, (1994).Characterization of oils extracted from wild-gathered tropical plant seeds Nigeria. Journal of American oil Content. 75 (8): 1031-1035.

Ibironke AA, OlusolaOO, (2013). Phytochemical analysis and mineral element composition of ten medicinal plant seeds from South-West Nigeria. New York Science Journal. 6(9): 22-28.

KyariMZ, (2008). Extraction and characterization of seed oils. International Agrophysics. 22: 139-142.

Mitra P,Ramaswamy HS, Chang KS, (2009). Pumpkin (Cucurbita maxima) seed oil extraction using supercritical carbon dioxide and physicochemical properties of the oil. Journal of Food Engineering. 95: 208-213.

Mohammed MI, Hamza ZU, (2008). Physicochemical properties of oil extracted from sesamum indicum I.seeds grown in Jigawa State- Nigeria. Journal of Applied Science and Environment. 12 (2):99-101.

Muibat OB, Temitope LA, Deborah OA, AbdulKabir OO, (2011).Physicochemical properties and fatty acids profile of seed oil of Telfairia occidentalis Hook, F. International Journal of Basic & Applied Sciences.11(06): 9 – 14.

NIFOR, Nigeria Institute of Oil Research (1989).History, Activities and Achivements.2ndedn. Benin City, Nigeria. Pp. 26-28.

Odugemi T, (2006).Outlines and pictures of medicinal plants from Nigeria (Vol. 10).University of Lagos press. Lagos.

Okonkwo PC, Mukhtar B and Usman JG, (2013). Approach to evaluation of solvent extraction of oil from neem seed. International Journal of Applied Science and Technology. 3 (6):76-85.

Orisakeye OT, Ojo AA, (2013). Antimicrobial and antioxidant evaluation of various parts of Cola millenii K. Schum plant. African Journal of Pharmacy and Pharmacology. 7(48): 3019-3025.

Peter MD, Wilson LD, Elisha K, Abdulquadir I, Abubakar BL, (2013). Extraction and biodegradation of baobab (Adansoni adigitata) seeds oil by fungi (Aspergillus niger). Journal of National Science Research. 3(5): 128-136.

Ratsch C, (2005). The Encyclopedia of psychoactive plants: ethno pharmacology and its applications, Rochester, Vermont.

Shah M, Garg SK, (2014). Application of Full Factorial Design in Optimization of Solvent-Free Microwave Extraction of Ginger Essential Oil. Journal of Engineering. 2014(2014): Article ID 828606, 5 pages.http://dx.doi.org/10.1155/2014/828606.